3-benzyl-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

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Chemical Name:3-benzyl-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione
CAS No.:701285-04-3
Molecular Formula:C₄₁H₃₄N₄O₉S
Molecular Weight:758.808
Hs Code.:

Synonyms:3-benzyl-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

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Chemical Property of 3-benzyl-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

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Technology Process of 3-benzyl-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

There total 2 articles about 3-benzyl-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 701285-00-9
6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

: 100-39-0
benzyl bromide

: 701285-03-2
4-benzyloxy-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

: 701285-04-3
3-benzyl-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

Guidance literature:: 6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione; With silver carbonate; In benzene; at 80 ℃; for 2h;

benzyl bromide; In benzene; at 60 - 70 ℃; for 48h;
DOI:10.1081/NCN-120027817

Reference yield:

: 138612-37-0
6-methyl-2-methylthio-4(3H),7(8H)-pteridinedione

: 701285-04-3
3-benzyl-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

Guidance literature:: Multi-step reaction with 2 steps

1.1: (NH₄)2SO₄; hexamethyldisilazane / 6 h / Heating

1.2: 45 percent / BF₃-etherate / CH₂Cl₂ / 24 h / 20 °C

2.1: silver carbonate / benzene / 2 h / 80 °C

2.2: 61 percent / benzene / 48 h / 60 - 70 °C

With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane; silver carbonate; In benzene;
DOI:10.1081/NCN-120027817