4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane

Base Information

Chemical Name:4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane
CAS No.:950666-83-8
Molecular Formula:C₁₂H₁₉N₃
Molecular Weight:205.303
Hs Code.:

Synonyms:4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane

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Chemical Property of 4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane

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Technology Process of 4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane

There total 2 articles about 4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.4%

: 4318-37-0
1-Methylhomopiperazine

: 6959-47-3
2-chloromethylpyridine hydrochloride

: 950666-83-8
4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane

Guidance literature:: With sodium hydroxide; In water; at 0 - 20 ℃; for 72h; Inert atmosphere; Sealed tube;
DOI:10.1016/j.jcat.2019.03.019

Reference yield: 46.0%

: 4318-37-0
1-Methylhomopiperazine

: 1121-60-4
pyridine-2-carbaldehyde

: 950666-83-8
4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane

Guidance literature:: 1-Methylhomopiperazine; pyridine-2-carbaldehyde; With sodium tris(acetoxy)borohydride; In dichloromethane; for 12h;

With sodium hydrogencarbonate; In dichloromethane; water; for 0.25h;

With sodium hydride; In tetrahydrofuran; for 1.5h;
DOI:10.1039/d1dt00299f

Reference yield: 91.0%

: 950666-83-8
4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane

: nickel(II) perchlorate hexahydrate

: 143-66-8
sodium tetraphenyl borate

: 75-05-8,26809-02-9
acetonitrile

: [Ni^II(4-methyl-1-[(pyridin-2-yl)methyl]-1,4-diazepane)(CH₃CN)₃](BPh₄)₂

Guidance literature:: 4-methyl-1-(pyrid-2-ylmethyl)-1,4-diazacycloheptane; nickel(II) perchlorate hexahydrate; In methanol; at 25 ℃; for 0.5h;

sodium tetraphenyl borate; acetonitrile; In methanol; for 1h;
DOI:10.1039/d0dt03887c