N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester

Base Information

• Chemical Name: N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester
• CAS No.: 857870-45-2
• Molecular Formula: C₂₆H₂₀Cl₂IN₃O₅
• Molecular Weight: 652.272

Synonyms:N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester

Chemical Property of N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester

There total 1 articles about N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2,6-dichlorobenzoyl)-4-[6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester (857870-53-2) + methyl iodide (74-88-4) → N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester (857870-45-2)

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃;

Reference yield:

N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester (857870-45-2) + tert-Butyl acrylate (1663-39-4,25232-27-3) → N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-(2-t-butoxycarbonylethenyl)-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester (857870-63-4)

Guidance literature:

With triethylamine; palladium diacetate; In DMF (N,N-dimethyl-formamide); at 70 ℃; for 3h;

Reference yield:

N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester (857870-45-2) + 2-(Trimethylsilyl)ethanol (2916-68-9) + carbon monoxide (201230-82-2) → N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-(trimethylsilylethoxycarbonyl)-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester (857870-65-6)

Guidance literature:

With triethylamine; palladium diacetate; In DMF (N,N-dimethyl-formamide); at 50 ℃;

upstream raw materials:

N-(2,6-dichlorobenzoyl)-4-[6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester

methyl iodide

Downstream raw materials:

N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-(trimethylsilylethoxycarbonyl)-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester

N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-benzyloxycarbonyl-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester

N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-(2-t-butoxycarbonylethenyl)-2,4-quinazoline-dione-3-yl]-L-phenylalanine methylester

N-(2,6-dichlorobenzoyl)-4-[1-methyl-6-iodo-2,4-quinazoline-dione-3-yl]-L-phenylalanine

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