triphenylverdazylium p-toluenesulfonate

Base Information

• Chemical Name: triphenylverdazylium p-toluenesulfonate
• CAS No.: 85963-94-6
• Molecular Formula: C₇H₇O₃S*C₂₀H₁₇N₄
• Molecular Weight: 484.579
• Mol file: 85963-94-6.mol

Synonyms:triphenylverdazylium p-toluenesulfonate

Chemical Property of triphenylverdazylium p-toluenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of triphenylverdazylium p-toluenesulfonate

There total 4 articles about triphenylverdazylium p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

1,3,5-triphenylverdazyl (2154-65-6) + Toluene-4-sulfonic acid adamantan-1-yl ester (16200-57-0) + acetonitrile (75-05-8,26809-02-9) → adamantane (281-23-2) + 1-adamanthanol (768-95-6) + N-(1-adamantyl)acetamide (880-52-4) + 2,4,6-triphenyl-1--1,2,3,4-tetrahydro-1,2,4,5-tetrazine (85963-93-5) + triphenylverdazylium p-toluenesulfonate (85963-94-6) + 2,4,6-triphenylverdazyl (22459-57-0)

Guidance literature:

With water; for 480h; Product distribution; Rate constant; Mechanism; Ambient temperature; var. solvents, var. reaction partners; other objects -kinetic and energy data of ionization;

Reference yield: 52.0%

silver(I) 4-methylbenzenesulfonate (16836-95-6) + 2,4,6-triphenylverdazylium bromide (51940-11-5) → triphenylverdazylium p-toluenesulfonate (85963-94-6)

Guidance literature:

In acetonitrile; Ambient temperature;

Reference yield:

1,3,5-triphenylverdazyl (2154-65-6) + Toluene-4-sulfonic acid adamantan-1-yl ester (16200-57-0) → 1-Adamantan-1-yl-2,4,6-triphenyl-1,2,3,4-tetrahydro-[1,2,4,5]tetrazine (112543-88-1) + triphenylverdazylium p-toluenesulfonate (85963-94-6)

Guidance literature:

In various solvent(s); at 20 ℃; Rate constant; Kinetics; Thermodynamic data; mechanism; ΔH(excit), ΔS(excit); var. temp. and solvents; var. reagents; var. substituted triphenylverdazyls;

upstream raw materials:

1,3,5-triphenylverdazyl

Toluene-4-sulfonic acid adamantan-1-yl ester

silver(I) 4-methylbenzenesulfonate

2,4,6-triphenylverdazylium bromide

Downstream raw materials:

1,3,5-triphenyl-6-(2,4,6-triphenyl-1,2,3,4-tetrahydro-1,2,3,5-tetrazinyl)-5,6-dihydro-1,2,3,5-tetrazinium p-toluenesulfonate