(+/-)-2-methyl-2-phenyl-2-phosphoniatricyclo<3.3.1.1^3.7>decane-4,8-dione iodide

Base Information

• Chemical Name: (+/-)-2-methyl-2-phenyl-2-phosphoniatricyclo<3.3.1.1^3.7>decane-4,8-dione iodide
• CAS No.: 126412-52-0
• Molecular Formula: C₁₆H₁₈O₂P*I
• Molecular Weight: 400.196

Synonyms:(+/-)-2-methyl-2-phenyl-2-phosphoniatricyclo<3.3.1.1^3.7>decane-4,8-dione iodide

Chemical Property of (+/-)-2-methyl-2-phenyl-2-phosphoniatricyclo<3.3.1.1^3.7>decane-4,8-dione iodide

Chemical Property:

Purity/Quality:

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Technology Process of (+/-)-2-methyl-2-phenyl-2-phosphoniatricyclo<3.3.1.1^3.7>decane-4,8-dione iodide

There total 5 articles about (+/-)-2-methyl-2-phenyl-2-phosphoniatricyclo<3.3.1.1^3.7>decane-4,8-dione iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-phenyl-2-phosphatricyclo<3.3.1.13,7>decane-4,8-dione (122557-75-9) + methyl iodide (74-88-4) → (+/-)-2-methyl-2-phenyl-2-phosphoniatricyclo<3.3.1.13.7>decane-4,8-dione iodide (126412-52-0)

Guidance literature:

In benzene; at 45 ℃; for 2h;

Reference yield:

(S,S)-bicyclo[3.3.1]nonane-2,6-dione (36415-87-9) → (-)-(1R,3R,5R,7R)-2-methyl-2-phenyl-2-phosphoniatricyclo<3.3.1.13.7>decane-4,8-dione iodide (126412-52-0,126456-52-8)

Guidance literature:

Multi-step reaction with 3 steps

2: H₂O

3: benzene / 2 h / 45 °C

With water; In benzene;

Reference yield:

C23H31ClN2O2P(1+)*Cl(1-) (122557-72-6) → (-)-(1R,3R,5R,7R)-2-methyl-2-phenyl-2-phosphoniatricyclo<3.3.1.13.7>decane-4,8-dione iodide (126412-52-0,126456-52-8)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O

2: benzene / 2 h / 45 °C

With water; In benzene;

upstream raw materials:

2-phenyl-2-phosphatricyclo<3.3.1.1^3,7>decane-4,8-dione

methyl iodide

(-)-(1R,3R,5R,7R)-2-phenyl-2-phosphatricyclo<3.3.1.1^3.7>decane-4,8-dione

(S,S)-bicyclo[3.3.1]nonane-2,6-dione

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