dibutyl ((5-chloro-1,3-dimethyl-1H-pyrazole-4-carboxamido)-(phenyl)methyl)phosphonate

Base Information

Chemical Name:dibutyl ((5-chloro-1,3-dimethyl-1H-pyrazole-4-carboxamido)-(phenyl)methyl)phosphonate
CAS No.:1300734-60-4
Molecular Formula:C₂₁H₃₁ClN₃O₄P
Molecular Weight:455.922
Hs Code.:

Synonyms:dibutyl ((5-chloro-1,3-dimethyl-1H-pyrazole-4-carboxamido)-(phenyl)methyl)phosphonate

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Chemical Property of dibutyl ((5-chloro-1,3-dimethyl-1H-pyrazole-4-carboxamido)-(phenyl)methyl)phosphonate

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Technology Process of dibutyl ((5-chloro-1,3-dimethyl-1H-pyrazole-4-carboxamido)-(phenyl)methyl)phosphonate

There total 7 articles about dibutyl ((5-chloro-1,3-dimethyl-1H-pyrazole-4-carboxamido)-(phenyl)methyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27006-76-4
5-chloro-4-formyl-1,3-dimethylpyrazole

: 1300734-60-4
dibutyl ((5-chloro-1,3-dimethyl-1H-pyrazole-4-carboxamido)-(phenyl)methyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium permanganate

2.1: thionyl chloride

3.1: ammonium hydroxide

3.2: 0 - 25 °C

With ammonium hydroxide; potassium permanganate; thionyl chloride;
DOI:10.1002/jhet.591

Reference yield:

: 1038997-74-8
C₇H₈O₃S*C₁₅H₂₆NO₃P

: 27006-83-3
1,3-dimethyl-5-chloro-pyrazole-4-carbonyl chloride

: 1300734-60-4
dibutyl ((5-chloro-1,3-dimethyl-1H-pyrazole-4-carboxamido)-(phenyl)methyl)phosphonate

Guidance literature:: C₇H₈O₃S*C₁₅H₂₆NO₃P; With ammonium hydroxide;

1,3-dimethyl-5-chloro-pyrazole-4-carbonyl chloride; With triethylamine; In tetrahydrofuran; at 0 - 25 ℃;
DOI:10.1002/jhet.591

Reference yield:

: 1038997-69-1
C₂₂H₃₀NO₃P

: 1300734-60-4
dibutyl ((5-chloro-1,3-dimethyl-1H-pyrazole-4-carboxamido)-(phenyl)methyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: water

2.1: ammonium hydroxide

2.2: 0 - 25 °C

With ammonium hydroxide; In water;
DOI:10.1002/jhet.591