benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Base Information

Chemical Name:benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester
CAS No.:894094-76-9
Molecular Formula:C₃₁H₃₅N₃O₇S
Molecular Weight:593.701
Hs Code.:

benzenesulfonic acid 4-[2-<i>tert</i>-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Synonyms:benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

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Chemical Property of benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

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Technology Process of benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

There total 7 articles about benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 894094-75-8
benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

: 74-88-4
methyl iodide

: 894094-76-9
benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;
DOI:10.1016/j.tetlet.2006.03.024

Reference yield:

: 894094-68-9
2-(4-benzenesulfonyloxy)benzyl-3-(4-methoxy-phenyl)-2-methylaminopropionic acid methyl ester

: 894094-76-9
benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / Et₃N; HgCl₂ / dimethylformamide / 12 h / 20 °C

2: 98 percent / 0.25 h / 20 °C

3: 82 percent / aq. NaHCO₃ / dioxane / 12 h / 20 °C

4: 99 percent / K₂CO₃ / dimethylformamide / 0.25 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; triethylamine; mercury dichloride; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.03.024

Reference yield:

: 894094-67-8
2-(4-benzenesulfonyloxy-benzyl)-2-(tert-butoxycarbonyl-methylamino)-3-(4-methoxy-phenyl)-propionic acid methyl ester

: 894094-76-9
benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-1,3-dimethyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / TFA / CH₂Cl₂ / 0 - 20 °C

2: 75 percent / Et₃N; HgCl₂ / dimethylformamide / 12 h / 20 °C

3: 98 percent / 0.25 h / 20 °C

4: 82 percent / aq. NaHCO₃ / dioxane / 12 h / 20 °C

5: 99 percent / K₂CO₃ / dimethylformamide / 0.25 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; triethylamine; trifluoroacetic acid; mercury dichloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.03.024