dodecafluoro-5,10-o-benzenostibanthrene

Base Information

• Chemical Name: dodecafluoro-5,10-o-benzenostibanthrene
• CAS No.: 59807-80-6
• Molecular Formula: C₁₈F₁₂Sb₂
• Molecular Weight: 687.679
• Mol file: 59807-80-6.mol

Synonyms:dodecafluoro-5,10-o-benzenostibanthrene

Chemical Property of dodecafluoro-5,10-o-benzenostibanthrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dodecafluoro-5,10-o-benzenostibanthrene

There total 1 articles about dodecafluoro-5,10-o-benzenostibanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

antimony (7440-36-0) + 5,6-diiodo-1,2,3,4-tetrafluorobenzene (2708-97-6) → antimony triiodide (7790-44-5) + dodecafluoro-5,10-o-benzenostibanthrene (59807-80-6)

Guidance literature:

In neat (no solvent); powd. Sb and I2C6F4 heated in sealed tube at 250°C overnight; solid crushed, extd. (petroleum ether), boiled with charcoal, crystals dried at 140°C (vac.) for 10-20 min; elem. anal.;

DOI:10.1016/0022-328X(84)80654-3

Reference yield:

dodecafluoro-5,10-o-benzenostibanthrene (59807-80-6) → dodecafluoro-5,10-o-benzenostibanthrene*0.5benzene

Guidance literature:

With benzene; In benzene; pptd. from concd. C6H6 soln.; elem. anal.;

DOI:10.1016/0022-328X(84)80654-3

Reference yield:

dodecafluoro-5,10-o-benzenostibanthrene (59807-80-6) → 2Sb(5+)*3C6F4(2-)*2OH(1-)*2NO3(1-)=Sb2(C6F4)3(OH)2(NO3)2

Guidance literature:

With nitric acid; In nitric acid; Sb2(C6F4)3 dissolved in boiling concd. HNO3; diluted with H2O, filtered, set aside for 2 d at room temp. or overnight in refrigerator, washed with cold H2O, dried at room temp. (vac.); elem. anal.;

DOI:10.1016/0022-328X(84)80654-3

upstream raw materials:

antimony

5,6-diiodo-1,2,3,4-tetrafluorobenzene

Downstream raw materials:

perfluoroselenanthrene