Technology Process of ethyl 6-(benzenesulphonylmethyl)-3-(furan-3-yl)-2-hydroxybenzoate
There total 6 articles about ethyl 6-(benzenesulphonylmethyl)-3-(furan-3-yl)-2-hydroxybenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron tribromide / dichloromethane / -70 - 20 °C
2: potassium fluoride monohydrate; sodium bromide / tetrakis(triphenylphosphine) palladium(0) / α,α,α-trifluorotoluene / 0.5 h / 175 °C / Microwave
With
potassium fluoride monohydrate; boron tribromide; sodium bromide;
tetrakis(triphenylphosphine) palladium(0);
In
dichloromethane; α,α,α-trifluorotoluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 50 °C
2: dihydrogen peroxide / water; acetic acid / 2 h / 60 °C
3: boron tribromide / dichloromethane / -70 - 20 °C
4: potassium fluoride monohydrate; sodium bromide / tetrakis(triphenylphosphine) palladium(0) / α,α,α-trifluorotoluene / 0.5 h / 175 °C / Microwave
With
potassium fluoride monohydrate; dihydrogen peroxide; boron tribromide; potassium carbonate; sodium bromide;
tetrakis(triphenylphosphine) palladium(0);
In
dichloromethane; α,α,α-trifluorotoluene; water; acetic acid; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / acetone / 2 h / Reflux
2: N-Bromosuccinimide / 2,2'-azobis(isobutyronitrile) / dichloromethane / irradiated with a 500W tungsten filament lamp
3: potassium carbonate / N,N-dimethyl-formamide / 1 h / 50 °C
4: dihydrogen peroxide / water; acetic acid / 2 h / 60 °C
5: boron tribromide / dichloromethane / -70 - 20 °C
6: potassium fluoride monohydrate; sodium bromide / tetrakis(triphenylphosphine) palladium(0) / α,α,α-trifluorotoluene / 0.5 h / 175 °C / Microwave
With
N-Bromosuccinimide; potassium fluoride monohydrate; dihydrogen peroxide; boron tribromide; potassium carbonate; sodium bromide;
tetrakis(triphenylphosphine) palladium(0); 2,2'-azobis(isobutyronitrile);
In
dichloromethane; α,α,α-trifluorotoluene; water; acetic acid; N,N-dimethyl-formamide; acetone;
