(CO)3ReB₅H₁₀

Base Information

Chemical Name:(CO)3ReB₅H₁₀
CAS No.:98586-75-5
Molecular Formula:C₃H₁₀B₅O₃Re
Molecular Weight:334.373
Hs Code.:

Synonyms:(CO)3ReB₅H₁₀

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CO)3ReB₅H₁₀

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Technology Process of (CO)3ReB₅H₁₀

There total 1 articles about (CO)3ReB₅H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.4%

: 14285-68-8
decacarbonyldirhenium⁽⁰⁾

: 19624-22-7
pentaborane⁽⁹⁾

: 1333-74-0
hydrogen

: 17702-41-9
nido-decaborane

: 2-{Re(CO)5}B₅H₈

: 98586-75-5
(CO)3ReB₅H₁₀

Guidance literature:: In neat (no solvent); catalyst Ru/C (5%; 0.51mmol), Re2(CO)10 (4.22mmol), B5H9 (25mmol), H2 (pressure about 100atm), single-ended stainless-steel cylinder of seamless one-piece construction, equipped with a stainless-steel needle valve; 120-125°C, 14d;; distn. of volatile contents of cylinder into the vacuum line (48h), distn. of B5H9 into a -196°C U-trap; the -35°C U-trap contains a mixture of B10H14, 2-((CO)5Re)B5H8 and (CO)3ReB5H8; condensation of (CO)3ReB5H8 into a -10°C trap;;