cis-[Fe(η2-phenylhydrazine(-H))(1,2-bis(dimethylphosphino)ethane)2]Cl*tetrahydrofuran

Base Information

Chemical Name:cis-[Fe(η2-phenylhydrazine(-H))(1,2-bis(dimethylphosphino)ethane)2]Cl*tetrahydrofuran
CAS No.:1362816-45-2
Molecular Formula:C₄H₈O*C₁₈H₃₉FeN₂P₄*Cl
Molecular Weight:570.823
Hs Code.:

Synonyms:cis-[Fe(η2-phenylhydrazine(-H))(1,2-bis(dimethylphosphino)ethane)2]Cl*tetrahydrofuran

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Chemical Property of cis-[Fe(η2-phenylhydrazine(-H))(1,2-bis(dimethylphosphino)ethane)2]Cl*tetrahydrofuran

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Technology Process of cis-[Fe(η2-phenylhydrazine(-H))(1,2-bis(dimethylphosphino)ethane)2]Cl*tetrahydrofuran

There total 1 articles about cis-[Fe(η2-phenylhydrazine(-H))(1,2-bis(dimethylphosphino)ethane)2]Cl*tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 27316-95-6,60966-88-3
trans-[FeCl₂(1,2-bis(dimethylphosphino)ethane)2]

: 100-63-0
phenylhydrazine

: 1362816-45-2
cis-[Fe(η2-phenylhydrazine(-H))(1,2-bis(dimethylphosphino)ethane)2]Cl*tetrahydrofuran

Guidance literature:: With (CH₃)3COK; In tetrahydrofuran; under N2; addn. of potassium tert-butoxide to soln. of iron compd. and phenylhydrazine in THF, mixt. stored overnight; crystals filtered off, washed with THF, dried under vac.;
DOI:10.1021/ic2027225

Reference yield: 69.0%

: 1362816-45-2
cis-[Fe(η2-phenylhydrazine(-H))(1,2-bis(dimethylphosphino)ethane)2]Cl*tetrahydrofuran

: 143-66-8
sodium tetraphenyl borate

: 1362815-98-2
cis-[Fe(η2-phenylhydrazine(-H))(1,2-bis(dimethylphosphino)ethane)2](tetraphenylborate)

Guidance literature:: In ethanol; under inert atm.; soln. of iron compd. in EtOH added to soln. of sodium tetraphenylborate in EtOH; ppt. filtered off, washed with EtOH and MeOH, dried under vac.; elem. anal.;
DOI:10.1021/ic2027225