6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid

Base Information

Chemical Name:6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid
CAS No.:77016-01-4
Molecular Formula:C₁₅H₁₇Cl₂N₃O₄
Molecular Weight:374.224
Hs Code.:

Synonyms:6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid

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Chemical Property of 6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid

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Technology Process of 6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid

There total 3 articles about 6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 77015-98-6
6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-α-D-glucopyranosylbromid

: 77016-01-4
6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid

Guidance literature:: With tetraethylammonium chloride; In acetonitrile; for 0.166667h; Ambient temperature;

Reference yield:

: 77015-96-4
1,6-Anhydro-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranose

: 77016-01-4
6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄ / acetic acid / 20 h / Ambient temperature

2: 95 percent / TiBr₄ / CH₂Cl₂; toluene; ethyl acetate / 20 h

3: 95 percent / N(C₂H₅)4Cl / acetonitrile / 0.17 h / Ambient temperature

With sulfuric acid; tetraethylammonium chloride; titanium(IV) bromide; In dichloromethane; acetic acid; ethyl acetate; toluene; acetonitrile;

Reference yield:

: 77015-97-5
1,6-Di-O-acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-α-D-glucopyranose

: 77016-01-4
6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / TiBr₄ / CH₂Cl₂; toluene; ethyl acetate / 20 h

2: 95 percent / N(C₂H₅)4Cl / acetonitrile / 0.17 h / Ambient temperature

With tetraethylammonium chloride; titanium(IV) bromide; In dichloromethane; ethyl acetate; toluene; acetonitrile;