4-O-(2'-Amino-4'-chlor-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

Base Information

Chemical Name:4-O-(2'-Amino-4'-chlor-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin
CAS No.:77016-06-9
Molecular Formula:C₁₉H₃₇ClN₄O₉
Molecular Weight:500.977
Hs Code.:

4-O-(2'-Amino-4'-chlor-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

Synonyms:

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Chemical Property of 4-O-(2'-Amino-4'-chlor-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

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Technology Process of 4-O-(2'-Amino-4'-chlor-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

There total 5 articles about 4-O-(2'-Amino-4'-chlor-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₀H₅₉ClN₆O₁₅

: 77016-06-9
4-O-(2'-Amino-4'-chlor-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In 1,4-dioxane; acetic acid; Yield given;

Reference yield:

: 77016-01-4
6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-β-D-glucopyranosylchlorid

: 77016-06-9
4-O-(2'-Amino-4'-chlor-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Drierite, molecular sieve 4 Angstroem, Hg(CN)2 / 1.)CH₃CN, PhMe, 60 deg C, 2.) PhMe, CH₃CN, reflux

2: NaOCH₃ / acetonitrile; methanol

3: H₂, 3percent HCl / 10percent Pd/C / dioxane; acetic acid

With hydrogenchloride; calcium sulfate; 4 A molecular sieve; hydrogen; sodium methylate; mercury(II) cyanide; palladium on activated charcoal; In 1,4-dioxane; methanol; acetic acid; acetonitrile;

Reference yield:

: 77015-98-6
6-O-Acetyl-2-azido-3-O-benzyl-4-chlor-2,4-didesoxy-α-D-glucopyranosylbromid

: 77016-06-9
4-O-(2'-Amino-4'-chlor-2',4'-didesoxy-α-D-glucopyranosyl)-2-desoxy-6-O-(3''-desoxy-4''-C-methyl-3''-methylamino-β-L-arabinopyranosyl)-D-streptamin

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / N(C₂H₅)4Cl / acetonitrile / 0.17 h / Ambient temperature

2: 1.) Drierite, molecular sieve 4 Angstroem, Hg(CN)2 / 1.)CH₃CN, PhMe, 60 deg C, 2.) PhMe, CH₃CN, reflux

3: NaOCH₃ / acetonitrile; methanol

4: H₂, 3percent HCl / 10percent Pd/C / dioxane; acetic acid

With hydrogenchloride; calcium sulfate; 4 A molecular sieve; tetraethylammonium chloride; hydrogen; sodium methylate; mercury(II) cyanide; palladium on activated charcoal; In 1,4-dioxane; methanol; acetic acid; acetonitrile;