2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid

Base Information

Chemical Name:2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid
CAS No.:1012330-55-0
Molecular Formula:C₂₆H₃₃NO₅Si
Molecular Weight:467.637
Hs Code.:

Synonyms:2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid

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Chemical Property of 2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid

Chemical Property:

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Technology Process of 2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid

There total 1 articles about 2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1012330-49-2
2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole

: 124-38-9,18923-20-1
carbon dioxide

: 1012330-55-0
2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid

Guidance literature:: 2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2.5h;

carbon dioxide; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h; Further stages.;
DOI:10.1021/jm701210y

Reference yield: 94.0%

: 1012330-55-0
2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid

: 18107-18-1
diazomethyl-trimethyl-silane

: 1012330-56-1
methyl 2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylate

Guidance literature:: In methanol; hexane; toluene; at 20 ℃; for 0.166667h;
DOI:10.1021/jm701210y

Reference yield:

: 1012330-55-0
2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid

: 593-51-1
methylamine hydrochloride

: C₂₇H₃₆N₂O₄Si

Guidance literature:: 2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazole-5-carboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;

methylamine hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h; Further stages.;
DOI:10.1021/jm701210y