2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline

Base Information

• Chemical Name: 2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline
• CAS No.: 474817-79-3
• Molecular Formula: C₁₄H₁₄F₃NO
• Molecular Weight: 269.266
• Mol file: 474817-79-3.mol

Synonyms:2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline

Chemical Property of 2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline

Chemical Property:

Purity/Quality:

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Technology Process of 2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline

There total 1 articles about 2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

6-(cyclopent-1-en-1-yl)-2-methyl-aniline (235779-09-6) + trifluoroacetic anhydride (407-25-0) → 2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline (474817-79-3)

Guidance literature:

DOI:10.1023/A:1015074016576

Reference yield: 67.0%

2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline (474817-79-3) → 6-methyl-2-(tetrahydro-2-pyranyl)aniline

Guidance literature:

2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline; With ozone; In methanol; at 0 - 5 ℃; for 0.0833333h;

With sodium tetrahydroborate; In methanol; at -20 ℃; for 18h;

DOI:10.1023/A:1015074016576

Reference yield: 66.0%

methanol (67-56-1) + 2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline (474817-79-3) → N-[2-(5,5-dimethoxypentanoyl)-6-methylphenyl]-2,2,2-trifluoroacetamide

Guidance literature:

methanol; 2-(cyclopent-1-en-1-yl)-6-methyl-N-trifluoroacetylaniline; With ozone; In methanol; at 0 - 5 ℃; for 0.0833333h;

With dimethylsulfide; In methanol; at 0 - 5 ℃; for 48h;

DOI:10.1023/A:1015074016576

upstream raw materials:

6-(cyclopent-1-en-1-yl)-2-methyl-aniline

trifluoroacetic anhydride