methyl 3-({2-chloro-4-[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-ylmethoxy]benzoyl}(methyl)amino)benzoate

Base Information

Chemical Name:methyl 3-({2-chloro-4-[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-ylmethoxy]benzoyl}(methyl)amino)benzoate
CAS No.:933799-78-1
Molecular Formula:C₂₉H₂₅Cl₃N₂O₅
Molecular Weight:587.887
Hs Code.:

Synonyms:methyl 3-({2-chloro-4-[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-ylmethoxy]benzoyl}(methyl)amino)benzoate

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Chemical Property of methyl 3-({2-chloro-4-[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-ylmethoxy]benzoyl}(methyl)amino)benzoate

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Technology Process of methyl 3-({2-chloro-4-[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-ylmethoxy]benzoyl}(methyl)amino)benzoate

There total 7 articles about methyl 3-({2-chloro-4-[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-ylmethoxy]benzoyl}(methyl)amino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 933799-72-5
methyl 3-{2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-yl]methoxy}benzoylamino}benzoate

: 74-88-4
methyl iodide

: 933799-78-1
methyl 3-({2-chloro-4-[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-ylmethoxy]benzoyl}(methyl)amino)benzoate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2007.01.046

Reference yield:

: 933799-64-5
2-chloro-4-{[5-isopropyl-3-(2,6-dichlorophenyl)-isoxazol-4-yl]methoxy}benzoic acid

: 933799-78-1
methyl 3-({2-chloro-4-[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-ylmethoxy]benzoyl}(methyl)amino)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / cooling

2: tetrahydrofuran / 20 °C

3: 98 percent / sodium hydride / dimethylformamide / 12 h / 20 °C

With sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2007.01.046

Reference yield:

: 278597-32-3
3-(2,6-dichlorophenyl)-4-(3'-chloro-4'-formylphenoxy)-methyl-5-isopropyl-isoxazole

: 933799-78-1
methyl 3-({2-chloro-4-[3-(2,6-dichlorophenyl)-5-isopropylisoxazol-4-ylmethoxy]benzoyl}(methyl)amino)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 3 h / 20 °C

2: triethylamine / tetrahydrofuran / cooling

3: tetrahydrofuran / 20 °C

4: 98 percent / sodium hydride / dimethylformamide / 12 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydride; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmc.2007.01.046