C₃₅H₃₃NO₇

Base Information

• Chemical Name: C₃₅H₃₃NO₇
• CAS No.: 1070196-50-7
• Molecular Formula: C₃₅H₃₃NO₇
• Molecular Weight: 579.65
• Mol file: 1070196-50-7.mol

Synonyms:C₃₅H₃₃NO₇

Chemical Property of C₃₅H₃₃NO₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₃₃NO₇

There total 3 articles about C₃₅H₃₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

1-(3'-amino-4'-methoxyphenyl)-1-(3'',4'',5''-trimethoxyphenyl)ethylene (1070195-62-8) + vadimezan (117570-53-3) → C35H33NO7 (1070196-50-7)

Guidance literature:

With pyridine; di-tert-butyl dicarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield:

3,4,5-trimethoxyphenylmagnesium bromide (133095-91-7) → C35H33NO7 (1070196-50-7)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / -40 - 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / dichloromethane / 0.5 h / 20 °C

3: pyridine; di-tert-butyl dicarbonate / N,N-dimethyl-formamide / 24 h / 20 °C

With pyridine; di-tert-butyl dicarbonate; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

1-(3-amino-4-methoxyphenyl)ethan-1-one (6318-64-5) → C35H33NO7 (1070196-50-7)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / -40 - 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / dichloromethane / 0.5 h / 20 °C

3: pyridine; di-tert-butyl dicarbonate / N,N-dimethyl-formamide / 24 h / 20 °C

With pyridine; di-tert-butyl dicarbonate; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

upstream raw materials:

1-(3'-amino-4'-methoxyphenyl)-1-(3'',4'',5''-trimethoxyphenyl)ethylene

vadimezan

1-(3-amino-4-methoxyphenyl)ethan-1-one

3,4,5-trimethoxyphenylmagnesium bromide