N₅,1-bis(4-aminophenyl)-N₃-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide

Base Information

Chemical Name:N₅,1-bis(4-aminophenyl)-N₃-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide
CAS No.:1357616-67-1
Molecular Formula:C₂₅H₂₄N₆O₂
Molecular Weight:440.505
Hs Code.:

N<sub>5</sub>,1-bis(4-aminophenyl)-N<sub>3</sub>-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide

Synonyms:N₅,1-bis(4-aminophenyl)-N₃-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide

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Chemical Property of N₅,1-bis(4-aminophenyl)-N₃-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide

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Technology Process of N₅,1-bis(4-aminophenyl)-N₃-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide

There total 7 articles about N₅,1-bis(4-aminophenyl)-N₃-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1357616-72-8
C₃₅H₄₀N₆O₆

: 1357616-67-1
N₅,1-bis(4-aminophenyl)-N₃-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide

Guidance literature:: C₃₅H₄₀N₆O₆; With hydrogenchloride; In water; ethyl acetate; at 20 ℃;

With ammonia;
DOI:10.1016/j.ejmech.2011.12.031

Reference yield:

: 71026-66-9
N-(tert-butoxycarbonyl)-1,4-phenylenediamine

: 1357616-67-1
N₅,1-bis(4-aminophenyl)-N₃-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; sodium nitrite / methanol; water

2.1: silver carbonate / 1,4-dioxane / 24 h / 80 °C

3.1: sodium hydroxide / methanol / 20 °C / Inert atmosphere

3.2: pH 4

4.1: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5.1: tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride / water; ethyl acetate / 20 °C

With hydrogenchloride; silver carbonate; sodium hydroxide; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; methanol; water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.12.031

Reference yield:

: C₃₀H₃₃N₇O₆

: 1357616-67-1
N₅,1-bis(4-aminophenyl)-N₃-(2,3-dimethylphenyl)-1H-pyrazole-3,5-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: hydrogenchloride / water; ethyl acetate / 20 °C

With hydrogenchloride; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.12.031