N,N,N-trimethyl-4-(trifluoromethyl)benzeneaminium trifluoromethanesulfonate

Base Information

Chemical Name:N,N,N-trimethyl-4-(trifluoromethyl)benzeneaminium trifluoromethanesulfonate
CAS No.:1246260-87-6
Molecular Formula:CF₃O₃S*C₁₀H₁₃F₃N
Molecular Weight:353.286
Hs Code.:

Synonyms:N,N,N-trimethyl-4-(trifluoromethyl)benzeneaminium trifluoromethanesulfonate

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Chemical Property of N,N,N-trimethyl-4-(trifluoromethyl)benzeneaminium trifluoromethanesulfonate

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Technology Process of N,N,N-trimethyl-4-(trifluoromethyl)benzeneaminium trifluoromethanesulfonate

There total 1 articles about N,N,N-trimethyl-4-(trifluoromethyl)benzeneaminium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 329-17-9
N,N-dimethyl-4-(trifluoromethyl)aniline

: 333-27-7
methyl trifluoromethanesulfonate

: 1246260-87-6
N,N,N-trimethyl-4-(trifluoromethyl)benzeneaminium trifluoromethanesulfonate

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1021/ol1018739

Reference yield: 99.0%

: 1246260-87-6
N,N,N-trimethyl-4-(trifluoromethyl)benzeneaminium trifluoromethanesulfonate

: 17049-49-9
octylmagnesium bromide

: 725251-79-6
1-(trifluoromethyl)-4-octylbenzene

Guidance literature:: With iron(III)-acetylacetonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; at 60 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2013.09.039

Reference yield: 96.0%

: 110-91-8,99108-56-2
morpholine

: 1246260-87-6
N,N,N-trimethyl-4-(trifluoromethyl)benzeneaminium trifluoromethanesulfonate

: 113845-69-5
4-(4-trifluoromethylphenyl)morpholine

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride; sodium t-butanolate; In 1,4-dioxane; at 75 ℃; for 5h; Molecular sieve; Schlenk technique;
DOI:10.1039/c3ob41989d