N-(4-(3-(allyloxy)-4-fluorophenoxy)benzyl)-N-(2-methyl-3-nitrophenyl)amine

Base Information

Chemical Name:N-(4-(3-(allyloxy)-4-fluorophenoxy)benzyl)-N-(2-methyl-3-nitrophenyl)amine
CAS No.:448957-16-2
Molecular Formula:C₂₃H₂₁FN₂O₄
Molecular Weight:408.429
Hs Code.:

Synonyms:N-(4-(3-(allyloxy)-4-fluorophenoxy)benzyl)-N-(2-methyl-3-nitrophenyl)amine

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Chemical Property of N-(4-(3-(allyloxy)-4-fluorophenoxy)benzyl)-N-(2-methyl-3-nitrophenyl)amine

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Technology Process of N-(4-(3-(allyloxy)-4-fluorophenoxy)benzyl)-N-(2-methyl-3-nitrophenyl)amine

There total 7 articles about N-(4-(3-(allyloxy)-4-fluorophenoxy)benzyl)-N-(2-methyl-3-nitrophenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 862374-44-5
4-(3-(allyloxy)-4-fluorophenoxy)benzaldehyde

: 603-83-8
3-nitro-o-tolylamine

: 448957-16-2
N-(4-(3-(allyloxy)-4-fluorophenoxy)benzyl)-N-(2-methyl-3-nitrophenyl)amine

Guidance literature:: 4-(3-(allyloxy)-4-fluorophenoxy)benzaldehyde; 3-nitro-o-tolylamine; With acetic acid; In dichloromethane; at 20 ℃; for 4h;

With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/jm050205o

Reference yield:

: 448957-15-1
3-(allyloxy)-4-fluorophenol

: 448957-16-2
N-(4-(3-(allyloxy)-4-fluorophenoxy)benzyl)-N-(2-methyl-3-nitrophenyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 73 percent / K₂CO₃ / dimethylformamide / 14 h / 100 °C

2.1: AcOH / CH₂Cl₂ / 4 h / 20 °C

2.2: 88 percent / Na(OAc)3BH / CH₂Cl₂ / 12 h / 20 °C

With potassium carbonate; acetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050205o

Reference yield:

: 448957-14-0
3-(allyloxy)-4-fluorophenyl-4-methylbenzenesulfonate

: 448957-16-2
N-(4-(3-(allyloxy)-4-fluorophenoxy)benzyl)-N-(2-methyl-3-nitrophenyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 68 percent / aq. KOH / ethanol / 2 h / 90 °C

2.1: 73 percent / K₂CO₃ / dimethylformamide / 14 h / 100 °C

3.1: AcOH / CH₂Cl₂ / 4 h / 20 °C

3.2: 88 percent / Na(OAc)3BH / CH₂Cl₂ / 12 h / 20 °C

With potassium hydroxide; potassium carbonate; acetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050205o