5-Chloro-2-fluoronicotinic acid

Base Information

• Chemical Name: 5-Chloro-2-fluoronicotinic acid
• CAS No.: 884494-57-9
• Molecular Formula: C6H3ClFNO2
• Molecular Weight: 175.54
• Hs Code.: 2933399090
• Mol file: 884494-57-9.mol

Synonyms:5-CHLORO-2-FLUORONICOTINIC ACID;2-FLUORO-5-CHLORONICOTINIC ACID;5-Chloro-2-fluoro-3-pyridinecarboxylic acid

Chemical Property of 5-Chloro-2-fluoronicotinic acid

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.563
• Boiling Point: 308.18 °C at 760 mmHg
• PKA: 2.17±0.10(Predicted)
• Flash Point: 140.183 °C
• PSA: 50.19000
• Density: 1.577 g/cm³
• LogP: 1.57230

Purity/Quality:

99% ^*data from raw suppliers

5-Chloro-2-fluoronicotinicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Chloro-2-fluoronicotinic acid

There total 1 articles about 5-Chloro-2-fluoronicotinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-fluoro-5-chloropyridine (1480-65-5) + carbon dioxide (124-38-9,18923-20-1) → C6H3ClFNO2 (884494-57-9)

Guidance literature:

2-fluoro-5-chloropyridine; With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; In tetrahydrofuran; n-heptane; at -78 ℃; for 1h;

carbon dioxide; In tetrahydrofuran; n-heptane; at -78 - 20 ℃; for 0.666667h;

Reference yield:

C6H3ClFNO2 (884494-57-9) + 4-bromo-3-fluorophenol (121219-03-2) → C12H6BrClFNO3

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃;

upstream raw materials:

2-fluoro-5-chloropyridine

carbon dioxide

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