Technology Process of C52H51BF2N2O10
There total 4 articles about C52H51BF2N2O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine;
In
tetrahydrofuran;
at 45 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/jo2005654
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 5 h / 55 °C / Inert atmosphere
2: iodine; iodic acid / ethanol / 0.33 h / 60 °C
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 16 h / 45 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; iodic acid; triethylamine;
In
tetrahydrofuran; ethanol;
1: Sonogashira reaction / 3: Sonogashira reaction;
DOI:10.1021/jo2005654
- Guidance literature:
-
Multi-step reaction with 2 steps
1: iodine; iodic acid / ethanol / 0.33 h / 60 °C
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 16 h / 45 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; iodic acid; triethylamine;
In
tetrahydrofuran; ethanol;
2: Sonogashira reaction;
DOI:10.1021/jo2005654
