N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis(4-methylbenzenesulfonamide)

Base Information

Chemical Name:N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis(4-methylbenzenesulfonamide)
CAS No.:164529-65-1
Molecular Formula:C₂₁H₂₈N₄O₄S₂
Molecular Weight:464.61
Hs Code.:

Synonyms:N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis(4-methylbenzenesulfonamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis(4-methylbenzenesulfonamide)

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Technology Process of N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis(4-methylbenzenesulfonamide)

There total 1 articles about N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis(4-methylbenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 77429-97-1
N¹,N⁵-ditosyl-3-azapentane-1,5-diamine

: 107-13-1,25014-41-9
acrylonitrile

: 164529-65-1
N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis(4-methylbenzenesulfonamide)

Guidance literature:: In benzene; for 120h; Heating;
DOI:10.1002/hlca.19970800314

Reference yield: 55.0%

: 164529-65-1
N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis(4-methylbenzenesulfonamide)

: Methanesulfonic acid 2-{2-[(2-{2-[[2-(2-methanesulfonyloxy-ethoxy)-ethyl]-(toluene-4-sulfonyl)-amino]-ethoxy}-ethyl)-(toluene-4-sulfonyl)-amino]-ethoxy}-ethyl ester

: 3-[4,10,16,22-Tetrakis-(toluene-4-sulfonyl)-1,7,13-trioxa-4,10,16,19,22-pentaaza-cyclotetracos-19-yl]-propionitrile

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 50 ℃;
DOI:10.1016/0040-4039(95)00206-R

Reference yield:

: 164529-65-1
N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis(4-methylbenzenesulfonamide)

: 191986-41-1
N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis{N-[2-(2-hyroxyethoxy)ethyl]4-methylbenzenesulfonamide}

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / K₂CO₃, Cs₂CO₃, NaI / acetonitrile / 19 h / Heating

2: 97 percent / toluene-4-sulfonic acid monohydrate / methanol / 12 h / Ambient temperature

With potassium carbonate; caesium carbonate; toluene-4-sulfonic acid; sodium iodide; In methanol; acetonitrile;
DOI:10.1002/hlca.19970800314