6-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-(4-fluorophenyl)-2,3-dihydropyridazin-3-one

Base Information

Chemical Name:6-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-(4-fluorophenyl)-2,3-dihydropyridazin-3-one
CAS No.:1591827-45-0
Molecular Formula:C₂₇H₂₇FN₂O₂Si
Molecular Weight:458.607
Hs Code.:

Synonyms:6-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-(4-fluorophenyl)-2,3-dihydropyridazin-3-one

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Chemical Property of 6-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-(4-fluorophenyl)-2,3-dihydropyridazin-3-one

Chemical Property:

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Technology Process of 6-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-(4-fluorophenyl)-2,3-dihydropyridazin-3-one

There total 3 articles about 6-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-(4-fluorophenyl)-2,3-dihydropyridazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1591827-44-9
ethyl 5-((tert-butyldiphenylsilyl)oxy)-2-(4-fluorophenyl)-2-hydroxy-4-oxopentanoate

: 1591827-45-0
6-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-(4-fluorophenyl)-2,3-dihydropyridazin-3-one

Guidance literature:: With sodium hydrogencarbonate; hydrazine hydrate; In water; acetic acid;

Reference yield:

: 352-13-6
4-flourophenylmagnesium bromide

: 1591827-45-0
6-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-(4-fluorophenyl)-2,3-dihydropyridazin-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / tetrahydrofuran

2: acetic acid / Petroleum ether

3: hydrazine hydrate; sodium hydrogencarbonate / water; acetic acid

With hydrogenchloride; sodium hydrogencarbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; water; acetic acid; Petroleum ether;

Reference yield:

: 1813-94-1
ethyl 4-fluorobenzoylformate

: 1591827-45-0
6-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-(4-fluorophenyl)-2,3-dihydropyridazin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / Petroleum ether

2: hydrazine hydrate; sodium hydrogencarbonate / water; acetic acid

With sodium hydrogencarbonate; hydrazine hydrate; acetic acid; In water; acetic acid; Petroleum ether;