S-acetyl 5-phenylpentanethiol

Base Information

Chemical Name:S-acetyl 5-phenylpentanethiol
CAS No.:31150-72-8
Molecular Formula:C₁₃H₁₈OS
Molecular Weight:222.351
Hs Code.:

Synonyms:S-acetyl 5-phenylpentanethiol

Suppliers and Price of S-acetyl 5-phenylpentanethiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of S-acetyl 5-phenylpentanethiol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of S-acetyl 5-phenylpentanethiol

There total 8 articles about S-acetyl 5-phenylpentanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 10521-91-2
5-phenylpentan-1-ol

: 507-09-5
tiolacetic acid

: 31150-72-8
S-acetyl 5-phenylpentanethiol

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h;
DOI:10.1021/jm000149l

Reference yield:

: 17920-83-1,73850-25-6,28525-69-1
5-phenyl-4-pentenoic acid

: 31150-72-8
S-acetyl 5-phenylpentanethiol

Guidance literature:: Multi-step reaction with 5 steps

1: diethyl ether; methanol

2: DIBAL-H / CH₂Cl₂ / 0.5 h / 0 °C

3: H₂ / PtO₂ / methanol / 2585.7 Torr

4: NBS, Ph₃P / CH₂Cl₂ / 0.42 h / 0 - 20 °C

5: dimethylformamide / 2 h / 4A molecular sieves

With N-Bromosuccinimide; hydrogen; diisobutylaluminium hydride; triphenylphosphine; platinum(IV) oxide; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm960167w

Reference yield:

: 37464-85-0
methyl 5-phenylpent-4-enoate

: 31150-72-8
S-acetyl 5-phenylpentanethiol

Guidance literature:: Multi-step reaction with 4 steps

1: DIBAL-H / CH₂Cl₂ / 0.5 h / 0 °C

2: H₂ / PtO₂ / methanol / 2585.7 Torr

3: NBS, Ph₃P / CH₂Cl₂ / 0.42 h / 0 - 20 °C

4: dimethylformamide / 2 h / 4A molecular sieves

With N-Bromosuccinimide; hydrogen; diisobutylaluminium hydride; triphenylphosphine; platinum(IV) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm960167w