benzyl (1R,2S,3R,4R)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate

Base Information

Chemical Name:benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate
CAS No.:147490-65-1
Molecular Formula:C₃₅H₃₀O₈
Molecular Weight:578.618
Hs Code.:

Synonyms:benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate

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Technology Process of benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate

There total 1 articles about benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 98-88-4
benzoyl chloride

: 147524-45-6
benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate

: 147490-65-1
benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate

Guidance literature:: With pyridine; dmap; In chloroform; for 24h;

Reference yield: 89.0%

: 147490-65-1
benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate

: 147490-57-1
(1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 14h;

Reference yield:

: 147490-65-1
benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate

: 147490-53-7
benzyl 2-<2-<(1'R,2'S,3'R,4'R)-2',3'-dibenzoyloxy-4'-(benzoyloxymethyl)cyclopentyl>thiazole-4-carboxamido>-3-methylbut-2-enoate

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / H₂ / 10percent Pd-C / ethyl acetate / 14 h

2: (COCl)2, DMF / CH₂Cl₂ / ice-NaCl bath to r.t.

3: DMAP / CHCl₃ / 1.5 h

4: 76 percent / PBr₃ / dimethylformamide / 0.5 h / -7 °C

5: 1) 1 M NaOH / 1) DMSO, 0.75 h, 2) xylenes, reflux, 35 min

With dmap; sodium hydroxide; oxalyl dichloride; hydrogen; phosphorus tribromide; N,N-dimethyl-formamide; palladium on activated charcoal; In dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide;