benzyl (1R,2S,3R,4R)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate

Base Information

Chemical Name:benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate
CAS No.:147524-45-6
Molecular Formula:C₂₈H₂₆O₇
Molecular Weight:474.51
Hs Code.:

Synonyms:benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate

Chemical Property:

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Technology Process of benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate

There total 1 articles about benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 147490-55-9
t-4,t-5-dibenzoyloxycyclopentane-r-1,c-3-dicarboxylic acid anhydride

: 100-51-6,185532-71-2
benzyl alcohol

: 147524-45-6
benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate

: 147490-59-3
dibenzyl t-4,t-5-dibenzoyloxycyclopentane-r-1,c-3-dicarboxylate

Guidance literature:: With hydrogenchloride; sodium tetrahydroborate; Yield given. Multistep reaction. Yields of byproduct given; 1) DMF, 5 h, 2) CHCl₃, 1 h;

Reference yield: 90.0%

: 98-88-4
benzoyl chloride

: 147524-45-6
benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate

: 147490-65-1
benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyl-4-(benzoyloxymethyl)cyclopentane-1-carboxylate

Guidance literature:: With pyridine; dmap; In chloroform; for 24h;

Reference yield:

: 147524-45-6
benzyl (1R*,2S*,3R*,4R*)-2,3-dibenzoyloxy-4-(hydroxymethyl)cyclopentane-1-carboxylate

: 147490-52-6
benzyl 6β-<(1'R,2'S,3'R,4'R)-2',3'-dibenzoyloxy-4'-(benzoyloxymethyl)cyclopentane-1'-carboxamido>penicillanate 1β-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / pyridine, DMAP / CHCl₃ / 24 h

2: 89 percent / H₂ / 10percent Pd-C / ethyl acetate / 14 h

3: (COCl)2, DMF / CH₂Cl₂ / ice-NaCl bath to r.t.

4: DMAP / CHCl₃ / 1.5 h

With pyridine; dmap; oxalyl dichloride; hydrogen; N,N-dimethyl-formamide; palladium on activated charcoal; In dichloromethane; chloroform; ethyl acetate;