Technology Process of C63H75NO15
There total 4 articles about C63H75NO15 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C61H71N3O14; tiolacetic acid;
In
pyridine;
at 20 ℃;
for 240h;
Inert atmosphere;
With
sodium methylate;
In
methanol;
at 20 ℃;
for 5h;
Inert atmosphere;
In
methanol;
DOI:10.1016/j.carres.2011.03.008
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / 2 h / 20 °C / Inert atmosphere
2.1: trimethylsilyl trifluoromethanesulfonate / diethyl ether / 1 h / -10 - 20 °C / Inert atmosphere; Molecular sieve
3.1: lithium methanolate / methanol / 168 h / Inert atmosphere; Reflux
3.2: amberlite IR 120 (H+)
4.1: pyridine / 240 h / 20 °C / Inert atmosphere
4.2: 5 h / 20 °C / Inert atmosphere
4.3: amberlite IR 120 (H+)
With
trimethylsilyl trifluoromethanesulfonate; lithium methanolate;
In
pyridine; methanol; diethyl ether;
DOI:10.1016/j.carres.2011.03.008
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trimethylsilyl trifluoromethanesulfonate / diethyl ether / 1 h / -10 - 20 °C / Inert atmosphere; Molecular sieve
2.1: lithium methanolate / methanol / 168 h / Inert atmosphere; Reflux
2.2: amberlite IR 120 (H+)
3.1: pyridine / 240 h / 20 °C / Inert atmosphere
3.2: 5 h / 20 °C / Inert atmosphere
3.3: amberlite IR 120 (H+)
With
trimethylsilyl trifluoromethanesulfonate; lithium methanolate;
In
pyridine; methanol; diethyl ether;
DOI:10.1016/j.carres.2011.03.008
