2-(1-benzyl-4-methyl-pyrrolidin-3-yl)-3H-imidazo[5,1-f][1,2,4]triazin-4-one

Base Information

Chemical Name:2-(1-benzyl-4-methyl-pyrrolidin-3-yl)-3H-imidazo[5,1-f][1,2,4]triazin-4-one
CAS No.:1448717-97-2
Molecular Formula:C₁₇H₁₉N₅O
Molecular Weight:309.371
Hs Code.:

Synonyms:2-(1-benzyl-4-methyl-pyrrolidin-3-yl)-3H-imidazo[5,1-f][1,2,4]triazin-4-one

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Chemical Property of 2-(1-benzyl-4-methyl-pyrrolidin-3-yl)-3H-imidazo[5,1-f][1,2,4]triazin-4-one

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Technology Process of 2-(1-benzyl-4-methyl-pyrrolidin-3-yl)-3H-imidazo[5,1-f][1,2,4]triazin-4-one

There total 3 articles about 2-(1-benzyl-4-methyl-pyrrolidin-3-yl)-3H-imidazo[5,1-f][1,2,4]triazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.6%

: 1448717-96-1
3-[(1-benzyl-4-methyl-pyrrolidine-3-carbonyl)-amino]-3H-imidazole-4-carboxylic acid methyl ester

: 1448717-97-2
2-(1-benzyl-4-methyl-pyrrolidin-3-yl)-3H-imidazo[5,1-f][1,2,4]triazin-4-one

Guidance literature:: With ammonium hydroxide; ammonium acetate; In methanol; at 130 ℃; for 48h; Sealed tube;

Reference yield:

: 885958-71-4
(3RS,4RS)-1-benzyl-4-methyl-pyrrolidine-3-carboxylic acid

: 1448717-97-2
2-(1-benzyl-4-methyl-pyrrolidin-3-yl)-3H-imidazo[5,1-f][1,2,4]triazin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 4 h / 85 °C / Reflux

2: triethylamine / dichloromethane / 8 h / 0 - 20 °C

3: ammonium acetate; ammonium hydroxide / methanol / 48 h / 130 °C / Sealed tube

With ammonium hydroxide; thionyl chloride; ammonium acetate; triethylamine; In methanol; dichloromethane;

Reference yield:

: 1448718-30-6
C₁₃H₁₆ClNO

: 1448717-97-2
2-(1-benzyl-4-methyl-pyrrolidin-3-yl)-3H-imidazo[5,1-f][1,2,4]triazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 8 h / 0 - 20 °C

2: ammonium acetate; ammonium hydroxide / methanol / 48 h / 130 °C / Sealed tube

With ammonium hydroxide; ammonium acetate; triethylamine; In methanol; dichloromethane;