(S,S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-<1-(3,4-dichlorobenzyl)-2-methoxy-1-methylethyl>-amine

Base Information

Chemical Name:(S,S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-<1-(3,4-dichlorobenzyl)-2-methoxy-1-methylethyl>-amine
CAS No.:222733-20-2
Molecular Formula:C₂₅H₃₇Cl₂NO₂Si
Molecular Weight:482.566
Hs Code.:

Synonyms:(S,S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-<1-(3,4-dichlorobenzyl)-2-methoxy-1-methylethyl>-amine

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Chemical Property of (S,S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-<1-(3,4-dichlorobenzyl)-2-methoxy-1-methylethyl>-amine

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Technology Process of (S,S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-<1-(3,4-dichlorobenzyl)-2-methoxy-1-methylethyl>-amine

There total 4 articles about (S,S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-<1-(3,4-dichlorobenzyl)-2-methoxy-1-methylethyl>-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: (3,4-dichlorobenzyl)magnesium bromide

: (S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-(2-methoxy-1-methylethylidene)-amine

: 222733-20-2
(S,S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-<1-(3,4-dichlorobenzyl)-2-methoxy-1-methylethyl>-amine

Guidance literature:: With magnesium bromide; In diethyl ether; dichloromethane; for 22h; Ambient temperature;
DOI:10.1021/jo982222+

Reference yield:

: 20989-17-7
(2S)-2-phenylglycinol

: 222733-20-2
(S,S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-<1-(3,4-dichlorobenzyl)-2-methoxy-1-methylethyl>-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NEt₃, DMAP / CH₂Cl₂ / 21 h / Ambient temperature

2: 95 percent / MgSO₄ / benzene / 3 h / Ambient temperature

3: MgBr₂ / CH₂Cl₂

With dmap; magnesium sulfate; triethylamine; magnesium bromide; In dichloromethane; benzene;
DOI:10.1021/jo982222+

Reference yield:

: 120417-13-2
(S)-2-(tert-butyldimethylsilyloxy)-1-phenylethylamine

: 222733-20-2
(S,S)-<2-(tert-butyldimethylsilyloxy)-1-phenylethyl>-<1-(3,4-dichlorobenzyl)-2-methoxy-1-methylethyl>-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / MgSO₄ / benzene / 3 h / Ambient temperature

2: MgBr₂ / CH₂Cl₂

With magnesium sulfate; magnesium bromide; In dichloromethane; benzene;
DOI:10.1021/jo982222+