α-nitrato n-propyl phenyl ketone

Base Information

• Chemical Name: α-nitrato n-propyl phenyl ketone
• CAS No.: 127311-59-5
• Molecular Formula: C₁₀H₁₁NO₄
• Molecular Weight: 209.202
• Mol file: 127311-59-5.mol

Synonyms:α-nitrato n-propyl phenyl ketone

Chemical Property of α-nitrato n-propyl phenyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-nitrato n-propyl phenyl ketone

There total 2 articles about α-nitrato n-propyl phenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

propiophenone (495-40-9) → α-nitrato n-propyl phenyl ketone (127311-59-5) + benzoic acid (65-85-0,8013-63-6)

Guidance literature:

With thallium(III) nitrate; In acetic acid; for 8h; Heating;

DOI:10.1021/jo00300a016

Reference yield:

2-bromo-1-phenylbutan-1-one (877-35-0,73908-28-8) → α-nitrato n-propyl phenyl ketone (127311-59-5)

Guidance literature:

With silver nitrate; acetonitrile;

DOI:10.1021/ja01621a073

Reference yield:

α-nitrato n-propyl phenyl ketone (127311-59-5) → 1-phenyl-1,2-butanedione (3457-55-4)

Guidance literature:

With piperidine; diethyl ether;

DOI:10.1021/ja01621a073

upstream raw materials:

2-bromo-1-phenylbutan-1-one

propiophenone

Downstream raw materials:

1-phenyl-1,2-butanedione

Refernces