chloro(phenylmethyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) perchlorate - 2-propanol (1/0.5)

Base Information

• Chemical Name: chloro(phenylmethyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) perchlorate - 2-propanol (1/0.5)
• CAS No.: 94780-63-9
• Molecular Formula: 0C₃H₈O*C₄₅H₃₈ClIO₂OsP₃*ClO₄
• Molecular Weight: 1185.77

Synonyms:chloro(phenylmethyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) perchlorate - 2-propanol (1/0.5)

Chemical Property of chloro(phenylmethyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) perchlorate - 2-propanol (1/0.5)

Chemical Property:

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Technology Process of chloro(phenylmethyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) perchlorate - 2-propanol (1/0.5)

There total 2 articles about chloro(phenylmethyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) perchlorate - 2-propanol (1/0.5) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

(phenyliodophosphido)chlorodicarbonylbis(triphenylphosphine)osmium(II) (94780-59-3) + sodium perchlorate → chloro(phenylmethyliodophosphine)dicarbonylbis(triphenylphosphine)osmium(II) perchlorate - 2-propanol (1/0.5) (94780-63-9)

Guidance literature:

With CH₃I; In dichloromethane; isopropyl alcohol; byproducts: NaI; N2-atmosphere; addn. of MeI to suspn. of Os-complex in CH2Cl2; addn. ofNaClO4 in i-PrOH;; evapn. of CH2Cl2 under vac.; recrystn. from CH2Cl2/i-PrOH; elem. anal.;

Reference yield:

{Os(PIC6H5)Cl(CO)2(P(C6H5)3)2} (94780-59-3) + perchlorate(1-) (14797-73-0,1059018-91-5) + methyl iodide (74-88-4) → {Os(PCH3IC6H5)Cl(CO)2(P(C6H5)3)2}(1+)*ClO4(1-)={Os(PCH3IC6H5)Cl(CO)2(P(C6H5)3)2}ClO4 (94780-63-9)

Guidance literature:

In not given; pptn.; elem. anal.; detn. by IR and (1)-NMR;;

DOI:10.1016/0022-328X(84)80514-8

upstream raw materials:

{Os(PIC₆H₅)Cl(CO)2(P(C₆H₅)3)2}

perchlorate^(1-)

methyl iodide

(phenyliodophosphido)chlorodicarbonylbis(triphenylphosphine)osmium(II)

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