methyl (E)-3-(dimethylamino)-2-propenoate

Base Information

Chemical Name:methyl (E)-3-(dimethylamino)-2-propenoate
CAS No.:81790-25-2
Molecular Formula:C₁₉H₂₁NO₃
Molecular Weight:311.381
Hs Code.:

methyl (E)-3-(dimethylamino)-2-<p-(benzyloxy)phenyl>propenoate

Synonyms:methyl (E)-3-(dimethylamino)-2-propenoate

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Chemical Property of methyl (E)-3-(dimethylamino)-2-propenoate

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Technology Process of methyl (E)-3-(dimethylamino)-2-propenoate

There total 3 articles about methyl (E)-3-(dimethylamino)-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 68641-16-7
(4-benzyloxy-phenyl)-acetic acid methyl ester

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 81790-25-2
methyl (E)-3-(dimethylamino)-2-propenoate

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; at 200 ℃; for 12h;
DOI:10.1021/jo00136a005

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 81790-25-2
methyl (E)-3-(dimethylamino)-2-propenoate

Guidance literature:: Multi-step reaction with 3 steps

1: BF₃*OEt₂ / 12 h / Ambient temperature

2: anhydrous potassium carbonate / butan-2-one / 24 h / Heating

3: 89 percent / N,N,N',N'-tetramethylethylenediamine / 12 h / 200 °C

With N,N,N,N,-tetramethylethylenediamine; boron trifluoride diethyl etherate; potassium carbonate; In butanone;
DOI:10.1021/jo00136a005

Reference yield:

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 81790-25-2
methyl (E)-3-(dimethylamino)-2-propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: anhydrous potassium carbonate / butan-2-one / 24 h / Heating

2: 89 percent / N,N,N',N'-tetramethylethylenediamine / 12 h / 200 °C

With N,N,N,N,-tetramethylethylenediamine; potassium carbonate; In butanone;
DOI:10.1021/jo00136a005