(2-O-benzyl-3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:(2-O-benzyl-3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside
CAS No.:1425471-82-4
Molecular Formula:C₄₃H₄₉IO₉
Molecular Weight:836.761
Hs Code.:

Synonyms:(2-O-benzyl-3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of (2-O-benzyl-3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside

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Technology Process of (2-O-benzyl-3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside

There total 12 articles about (2-O-benzyl-3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1425471-79-9
(3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside

: 100-39-0
benzyl bromide

: 1425471-82-4
(2-O-benzyl-3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1002/anie.201206221

Reference yield:

: 1425471-76-6
p-iodophenyl (3-O-allyl-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-(4-O-benzyl-2-O-methyl)-α-L-rhamnopyranoside

: 1425471-82-4
(2-O-benzyl-3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium / 16 h / 20 °C

2: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

With methanol; sodium; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1002/anie.201206221

Reference yield:

: 1425471-60-8
p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside

: 1425471-82-4
(2-O-benzyl-3-O-allyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-p-iodophenyl 2-O-methyl-4-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-(phenylthio)-ε-caprolactam; 2,4,6-tri-tert-butylpyrimidine / dichloromethane; toluene / 0.33 h / 20 °C

1.2: -25 - 20 °C

2.1: methanol; sodium / 16 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

With methanol; N-(phenylthio)-ε-caprolactam; sodium; sodium hydride; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201206221