methyl 5-benzyloxy-2-hydroxy-6-methoxy-3-methylnaphthalene-1-carboxylate

Base Information

Chemical Name:methyl 5-benzyloxy-2-hydroxy-6-methoxy-3-methylnaphthalene-1-carboxylate
CAS No.:1437308-56-9
Molecular Formula:C₂₁H₂₀O₅
Molecular Weight:352.387
Hs Code.:

Synonyms:methyl 5-benzyloxy-2-hydroxy-6-methoxy-3-methylnaphthalene-1-carboxylate

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Chemical Property of methyl 5-benzyloxy-2-hydroxy-6-methoxy-3-methylnaphthalene-1-carboxylate

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Technology Process of methyl 5-benzyloxy-2-hydroxy-6-methoxy-3-methylnaphthalene-1-carboxylate

There total 5 articles about methyl 5-benzyloxy-2-hydroxy-6-methoxy-3-methylnaphthalene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: methyl 1-acetoxy-5-benzyloxy-6-methoxy-3-methyl-2-oxo-1,2,3,4-tetrahydronaphthalene-1-carboxylate

: 1437308-56-9
methyl 5-benzyloxy-2-hydroxy-6-methoxy-3-methylnaphthalene-1-carboxylate

Guidance literature:: With silica gel; In benzene; for 48h; Reflux;
DOI:10.1021/jo400737f

Reference yield: 83.0%

: 1437308-48-9
methyl 5-(2-benzyloxy-3-methoxyphenyl)-4-methyl-3-oxopentanoate

: 1437308-56-9
methyl 5-benzyloxy-2-hydroxy-6-methoxy-3-methylnaphthalene-1-carboxylate

Guidance literature:: methyl 5-(2-benzyloxy-3-methoxyphenyl)-4-methyl-3-oxopentanoate; With manganese triacetate; acetic acid;

With silica gel; In benzene; Reflux;
DOI:10.1021/jo400737f

Reference yield:

: 58402-40-7
2-(benzyloxy)-3-(bromomethyl)-1-methoxybenzene

: 1437308-56-9
methyl 5-benzyloxy-2-hydroxy-6-methoxy-3-methylnaphthalene-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 - 20 °C

1.2: 1.25 h / 0 °C

1.3: 1.5 h / 0 - 20 °C

2.1: acetic acid; manganese triacetate

2.2: Reflux

With manganese triacetate; sodium hydride; acetic acid; In tetrahydrofuran;
DOI:10.1021/jo400737f