N-(3,4-dichlorophenyl)pyrrolidine-1-carboximidothioic acid methyl ester

Base Information

Chemical Name:N-(3,4-dichlorophenyl)pyrrolidine-1-carboximidothioic acid methyl ester
CAS No.:1310682-80-4
Molecular Formula:C₁₂H₁₄Cl₂N₂S
Molecular Weight:289.229
Hs Code.:

Synonyms:N-(3,4-dichlorophenyl)pyrrolidine-1-carboximidothioic acid methyl ester

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Chemical Property of N-(3,4-dichlorophenyl)pyrrolidine-1-carboximidothioic acid methyl ester

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Technology Process of N-(3,4-dichlorophenyl)pyrrolidine-1-carboximidothioic acid methyl ester

There total 2 articles about N-(3,4-dichlorophenyl)pyrrolidine-1-carboximidothioic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 309942-79-8
pyrrolidine-1-carbothioic acid (3,4-dichlorophenyl)amide

: 74-88-4
methyl iodide

: 1310682-80-4
N-(3,4-dichlorophenyl)pyrrolidine-1-carboximidothioic acid methyl ester

Guidance literature:: pyrrolidine-1-carbothioic acid (3,4-dichlorophenyl)amide; methyl iodide; In acetone; at 60 ℃; for 4h; Inert atmosphere;

In tetrahydrofuran; water; at 25 ℃; Alkaline conditions; Inert atmosphere;
DOI:10.1021/jm200111g

Reference yield:

: 6590-94-9
3,4-dichlorophenyl isothiocyanate

: 1310682-80-4
N-(3,4-dichlorophenyl)pyrrolidine-1-carboximidothioic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 2 h / 25 °C / Inert atmosphere

2.1: acetone / 4 h / 60 °C / Inert atmosphere

2.2: 25 °C / Alkaline conditions; Inert atmosphere

In dichloromethane; acetone;
DOI:10.1021/jm200111g