ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate

Base Information

• Chemical Name: ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate
• CAS No.: 337519-90-1
• Molecular Formula: C₂₁H₂₉F₃N₂O₇S
• Molecular Weight: 510.532

Synonyms:ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate

Chemical Property of ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate

Chemical Property:

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Technology Process of ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate

There total 1 articles about ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

ethyl 2-(chlorosulfonyl)acetate (55896-93-0) + ethyl acetate (141-78-6) + 4-[(N-(t-butoxycarbonyl)piperidin-4-yl)oxy]-3-trifluoromethylbenzenamine (325457-62-3) → ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate (337519-90-1)

Guidance literature:

With pyridine; In hexane; dichloromethane;

Reference yield: 93.0%

ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate (337519-90-1) + 3-(3-cyanophenyl)-2-(E)-propen-1-ol (98116-50-8) → ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]-N-[3-(3-cyanophenyl)-2-(E)-propenyl]sulfamoylacetate (337521-71-8)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield: 93.0%

ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]sulfamoylacetate (337519-90-1) + ethyl acetate (141-78-6) + diethylazodicarboxylate (1972-28-7,218603-74-8) + 3-(3-cyanophenyl)-2-(E)-propen-1-ol (98116-50-8) → ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]-N-[3-(3-cyanophenyl)-2-(E)-propenyl]sulfamoylacetate (337521-71-8)

Guidance literature:

With triphenylphosphine; In dichloromethane;

upstream raw materials:

ethyl 2-(chlorosulfonyl)acetate

ethyl acetate

4-[(N-(t-butoxycarbonyl)piperidin-4-yl)oxy]-3-trifluoromethylbenzenamine

Downstream raw materials:

ethyl N-[4-(1-t-butoxycarbonylpiperidin-4-yloxy)-3-trifluoromethylphenyl]-N-[3-(3-cyanophenyl)-2-(E)-propenyl]sulfamoylacetate

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