carbonyl(benzonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate

Base Information

Chemical Name:carbonyl(benzonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate
CAS No.:133672-19-2
Molecular Formula:C₂₀H₃₇MnNOP₄*C₂₄H₂₀B
Molecular Weight:805.587
Hs Code.:

Synonyms:carbonyl(benzonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate

Suppliers and Price of carbonyl(benzonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of carbonyl(benzonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of carbonyl(benzonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate

There total 2 articles about carbonyl(benzonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 133672-21-6
carbonyl(acetonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate

: 100-47-0
benzonitrile

: 133672-19-2
carbonyl(benzonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate

: 75-05-8,26809-02-9
acetonitrile

Guidance literature:: In benzonitrile; at 70°C for 1.5 h; added diethyl ether; pptd.;
DOI:10.1021/om00051a020

Reference yield: 60.0%

: trans-dimethylbis(1,2-bis(dimethylphosphino)ethane)manganese(III) tetraphenylborate

: 100-47-0
benzonitrile

: 133672-19-2
carbonyl(benzonitrile)bis(1,2-bis(dimethylphosphino)ethane)manganese(I) tetraphenylborate

Guidance literature:: With CO; In benzonitrile; byproducts: acetone, CH4, C2H6; (N2); introduced CO to soln. of Mn-complex at room temp. at atmospheric pressure; heated to 90°C for 3 h; added ether; recrystd. from THF/ether at -30°C; elem. anal., GC;
DOI:10.1021/om00051a020