ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane

Base Information

Chemical Name:ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane
CAS No.:126380-11-8
Molecular Formula:C₂₈H₃₆N₂O₅
Molecular Weight:480.604
Hs Code.:

Synonyms:ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane

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Technology Process of ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane

There total 5 articles about ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.2%

: 4391-98-4
ethyl 4-ethyl-3-methylpyrrole-2-carboxylate

: 123-11-5
4-methoxy-benzaldehyde

: 126380-11-8
ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane

Guidance literature:: With hydrogenchloride; In methanol; water; for 4h; Reflux;
DOI:10.1134/S1070363215030196

Reference yield:

: 2199-47-5
ethyl 3,5-dimethyl-4-ethylpyrrole-2-carboxylate

: 126380-11-8
ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sulfuryl chloride, 2.) sodium acetate / 1.) ether, room temp., 12 h, 2.) acetone, water, reflux, 2 h

2: 72 percent / iodine, potassium iodide / ethanol; H₂O / 0.17 h / 60 °C

3: SnCl₂*2H₂O, potassium iodide, HCl / ethanol / 0.5 h / Heating

4: HCl / ethanol / 2.5 h / Heating

With hydrogenchloride; sulfuryl dichloride; iodine; sodium acetate; potassium iodide; tin(ll) chloride; In ethanol; water;

Reference yield:

: 53365-89-2
5-Ethoxycarbonyl-3-ethyl-4-methylpyrrole-2-carboxylic acid

: 126380-11-8
ms-(4''-methoxyphenyl)-5,5'-dicarbethoxy-4,4'-dimethyl-3,3'-diethyldipyrrolylmethane

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / iodine, potassium iodide / ethanol; H₂O / 0.17 h / 60 °C

2: SnCl₂*2H₂O, potassium iodide, HCl / ethanol / 0.5 h / Heating

3: HCl / ethanol / 2.5 h / Heating

With hydrogenchloride; iodine; potassium iodide; tin(ll) chloride; In ethanol; water;