2-(4-(5-chloro-2-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,3-dioxaborolane

Base Information

Chemical Name:2-(4-(5-chloro-2-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,3-dioxaborolane
CAS No.:1437034-72-4
Molecular Formula:C₁₈H₁₉BClFO₃
Molecular Weight:348.609
Hs Code.:

Synonyms:2-(4-(5-chloro-2-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,3-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-(5-chloro-2-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,3-dioxaborolane

Chemical Property:

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Technology Process of 2-(4-(5-chloro-2-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,3-dioxaborolane

There total 1 articles about 2-(4-(5-chloro-2-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,3-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 696-02-6
4-chloro-1,2-difluorobenzene

: 269409-70-3
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

: 1437034-72-4
2-(4-(5-chloro-2-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,3-dioxaborolane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 12h;

Reference yield:

: 1437034-72-4
2-(4-(5-chloro-2-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,3-dioxaborolane

: 1437034-74-6
2-chloro-6-vinylpyrimidine-4-carboxylic acid

: 1437034-76-8
C₁₉H₁₂ClFN₂O₃

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; caesium carbonate; In 1,2-dimethoxyethane; ethanol; water; at 95 ℃; for 4h; Sealed tube;

Reference yield:

: 1437034-72-4
2-(4-(5-chloro-2-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,3-dioxaborolane

: 1437034-25-7
(R)-2-(4-(5-chloro-2-fluorophenoxy)phenyl)-6-(1,2-dihydroxyethyl)pyrimidine-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethanol; water; 1,2-dimethoxyethane / 4 h / 95 °C / Sealed tube

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; ammonium carbonate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

3: AD-mix β; water / isopropyl alcohol / 48 h / 0 - 20 °C

With bis-triphenylphosphine-palladium(II) chloride; AD-mix β; water; ammonium carbonate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; isopropyl alcohol;