3,3'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(1,5-diphenyl-4,5-dihydro-1H-pyrazole)

Base Information

• Chemical Name: 3,3'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(1,5-diphenyl-4,5-dihydro-1H-pyrazole)
• CAS No.: 1364309-47-6
• Molecular Formula: C₄₁H₃₆N₆
• Molecular Weight: 612.777

Synonyms:3,3'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(1,5-diphenyl-4,5-dihydro-1H-pyrazole)

Chemical Property of 3,3'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(1,5-diphenyl-4,5-dihydro-1H-pyrazole)

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Technology Process of 3,3'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(1,5-diphenyl-4,5-dihydro-1H-pyrazole)

There total 4 articles about 3,3'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(1,5-diphenyl-4,5-dihydro-1H-pyrazole) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1,1'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(3-phenylprop-2-en-1-one) (1364309-66-9) + phenylhydrazine (100-63-0) → 3,3'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(1,5-diphenyl-4,5-dihydro-1H-pyrazole) (1364309-47-6)

Guidance literature:

With acetic acid; In ethanol; at 60 ℃; for 0.116667h; Microwave irradiation;

DOI:10.1002/jccs.201190137

Reference yield:

acetylacetone (123-54-6,81235-32-7) → 3,3'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(1,5-diphenyl-4,5-dihydro-1H-pyrazole) (1364309-47-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium ethanolate / ethanol / 20 °C

2: sodium hydroxide / ethanol; water / 0.07 h / 60 °C / Microwave irradiation

3: acetic acid / ethanol / 0.12 h / 60 °C / Microwave irradiation

With sodium ethanolate; acetic acid; sodium hydroxide; In ethanol; water;

DOI:10.1002/jccs.201190137

Reference yield:

1-chloro-1-(p-tolylhydrazone)propanone (132815-80-6,18440-55-6) → 3,3'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(1,5-diphenyl-4,5-dihydro-1H-pyrazole) (1364309-47-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium ethanolate / ethanol / 20 °C

2: sodium hydroxide / ethanol; water / 0.07 h / 60 °C / Microwave irradiation

3: acetic acid / ethanol / 0.12 h / 60 °C / Microwave irradiation

With sodium ethanolate; acetic acid; sodium hydroxide; In ethanol; water;

DOI:10.1002/jccs.201190137

upstream raw materials:

1,1'-(5-methyl-1-(4-tolyl)-1H-pyrazole-3,4-diyl)bis(3-phenylprop-2-en-1-one)

phenylhydrazine

1-chloro-1-(p-tolylhydrazone)propanone

3,4-diacetyl-5-methyl-1-(4-methylphenyl)-1H-pyrazole

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