2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol

Base Information

Chemical Name:2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol
CAS No.:776306-90-2
Molecular Formula:C₁₅H₂₆O₂
Molecular Weight:238.37
Hs Code.:

Synonyms:2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol

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Chemical Property of 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol

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Technology Process of 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol

There total 1 articles about 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 776306-89-9
methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate

: 776306-90-2
2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 2h;
DOI:10.1016/j.tetlet.2004.07.103

Reference yield: 76.0%

: 776306-90-2
2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol

: 776306-91-3
2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2004.07.103

Reference yield:

: 776306-90-2
2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol

: 776306-92-4
(1S,5R,6R)-5-isopropenyl-6-(4-methoxy-2-methylbut-3-en-2-yl)-2-methyl-cyclohex-2-enyl methyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / PCC; NaOAc / CH₂Cl₂ / 1 h / 20 °C

2: 71 percent / K(+)tAmO(-) / tetrahydrofuran / 3 h / 20 °C

With sodium acetate; potassium 2,2-dimethyl-1-propanolate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2004.07.103