methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate

Base Information

Chemical Name:methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate
CAS No.:776306-89-9
Molecular Formula:C₁₆H₂₆O₃
Molecular Weight:266.381
Hs Code.:

Synonyms:methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate

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Chemical Property of methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate

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Technology Process of methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate

There total 1 articles about methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 74-88-4
methyl iodide

: 776306-88-8
methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]propionate

: 776306-89-9
methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate

Guidance literature:: methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]propionate; With 4-hydroxymethyl-3-methoxyphenoxyacetic acid; lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 ℃; for 1h;

methyl iodide; In tetrahydrofuran; hexane; at 20 ℃; for 6h;

Reference yield: 86.0%

: 776306-89-9
methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate

: 776306-90-2
2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 2h;
DOI:10.1016/j.tetlet.2004.07.103

Reference yield:

: 776306-89-9
methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate

: 776306-91-3
2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / LAH / diethyl ether / 2 h / 0 °C

2: 76 percent / PCC; NaOAc / CH₂Cl₂ / 1 h / 20 °C

With lithium aluminium tetrahydride; sodium acetate; pyridinium chlorochromate; In diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2004.07.103