2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal

Base Information

• Chemical Name: 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal
• CAS No.: 776306-91-3
• Molecular Formula: C₁₅H₂₄O₂
• Molecular Weight: 236.354

Synonyms:2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal

Chemical Property of 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal

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Technology Process of 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal

There total 2 articles about 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol (776306-90-2) → 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal (776306-91-3)

Guidance literature:

With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2004.07.103

Reference yield:

methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate (776306-89-9) → 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal (776306-91-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / LAH / diethyl ether / 2 h / 0 °C

2: 76 percent / PCC; NaOAc / CH₂Cl₂ / 1 h / 20 °C

With lithium aluminium tetrahydride; sodium acetate; pyridinium chlorochromate; In diethyl ether; dichloromethane;

DOI:10.1016/j.tetlet.2004.07.103

Reference yield: 71.0%

(methoxymethyl)triphenylphosphonium chloride (4009-98-7) + 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanal (776306-91-3) → (1S,5R,6R)-5-isopropenyl-6-(4-methoxy-2-methylbut-3-en-2-yl)-2-methyl-cyclohex-2-enyl methyl ether (776306-92-4)

Guidance literature:

With potassium 2,2-dimethyl-1-propanolate; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1016/j.tetlet.2004.07.103

upstream raw materials:

2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methylpropanol

methyl 2-[(1S,2R,6R)-6-isopropenyl-2-methoxy-3-methyl-cyclohex-3-enyl]-2-methyl-propionate

Downstream raw materials:

(1S,5R,6R)-5-isopropenyl-6-(4-methoxy-2-methylbut-3-en-2-yl)-2-methyl-cyclohex-2-enyl methyl ether

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