N-[2-(4-chlorophenyl)-2-(4-chlorophenylamino)ethyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-[2-(4-chlorophenyl)-2-(4-chlorophenylamino)ethyl]-4-methylbenzenesulfonamide
CAS No.:1269423-64-4
Molecular Formula:C₂₁H₂₀Cl₂N₂O₂S
Molecular Weight:435.374
Hs Code.:

Synonyms:N-[2-(4-chlorophenyl)-2-(4-chlorophenylamino)ethyl]-4-methylbenzenesulfonamide

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Chemical Property of N-[2-(4-chlorophenyl)-2-(4-chlorophenylamino)ethyl]-4-methylbenzenesulfonamide

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Technology Process of N-[2-(4-chlorophenyl)-2-(4-chlorophenylamino)ethyl]-4-methylbenzenesulfonamide

There total 4 articles about N-[2-(4-chlorophenyl)-2-(4-chlorophenylamino)ethyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 106-47-8
4-chloro-aniline

: 97401-93-9
N-(p-toluenesulfonyl)-2-(4-chlorophenyl)aziridine

: 1269423-64-4
N-[2-(4-chlorophenyl)-2-(4-chlorophenylamino)ethyl]-4-methylbenzenesulfonamide

Guidance literature:: With [Ag(COD)2](+)PF₆(-); In 1,1-dichloroethane; at 20 ℃; for 3h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo102285z

Reference yield:

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 1269423-64-4
N-[2-(4-chlorophenyl)-2-(4-chlorophenylamino)ethyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: phenyltrimethylammonium tribromide / acetonitrile / 12 h / 20 °C / Inert atmosphere

2: [Ag(COD)2](+)PF₆(-) / 1,1-dichloroethane / 3 h / 20 °C / Inert atmosphere

With [Ag(COD)2](+)PF₆(-); phenyltrimethylammonium tribromide; In 1,1-dichloroethane; acetonitrile;
DOI:10.1021/jo102285z

Reference yield:

: 55962-05-5
[N-(p-tolylsulfonyl)imino]phenyliodinane

: 1269423-64-4
N-[2-(4-chlorophenyl)-2-(4-chlorophenylamino)ethyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: [Cu₃(benzene 1,3,5-tricarboxylate)₂(H₂O)₃]_n thermal activated at 120 °C / acetonitrile / 2 h / 20 °C / Molecular sieve; Inert atmosphere

2: [Cu₃(benzene 1,3,5-tricarboxylate)₂(H₂O)₃]_n thermal activated at 120 °C / acetonitrile / 10 h / 20 °C / Inert atmosphere; Glovebox; Schlenk technique

With [Cu₃(benzene 1,3,5-tricarboxylate)₂(H₂O)₃]_n thermal activated at 120 °C; In acetonitrile;
DOI:10.1021/acs.inorgchem.1c00201