Technology Process of 6,7-di(3-benzyloxy-4-methoxyphenyl)-6,7-dehydroindolizidine
There total 9 articles about 6,7-di(3-benzyloxy-4-methoxyphenyl)-6,7-dehydroindolizidine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / Na / benzene; diethyl ether / 5 h / Heating
2: 91 percent / AcONa / ethanol / 7 h / Heating
3: alkaline hydrolysis
4: 50 percent / methanol; H2O / 48 h / Ambient temperature; phosphate buffer, pH ca. 7.0
5: 2.) NaBH4 / 1.) MeOH, room temp., 12 h, 2.) C6H6, 2 h
With
sodium tetrahydroborate; sodium acetate; sodium;
In
methanol; diethyl ether; ethanol; water; benzene;
DOI:10.1016/0040-4020(80)80227-4
- Guidance literature:
-
Multi-step reaction with 3 steps
1: alkaline hydrolysis
2: 50 percent / methanol; H2O / 48 h / Ambient temperature; phosphate buffer, pH ca. 7.0
3: 2.) NaBH4 / 1.) MeOH, room temp., 12 h, 2.) C6H6, 2 h
With
sodium tetrahydroborate;
In
methanol; water;
DOI:10.1016/0040-4020(80)80227-4
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 91 percent / AcONa / ethanol / 7 h / Heating
2: alkaline hydrolysis
3: 50 percent / methanol; H2O / 48 h / Ambient temperature; phosphate buffer, pH ca. 7.0
4: 2.) NaBH4 / 1.) MeOH, room temp., 12 h, 2.) C6H6, 2 h
With
sodium tetrahydroborate; sodium acetate;
In
methanol; ethanol; water;
DOI:10.1016/0040-4020(80)80227-4
