(E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide

Base Information

Chemical Name:(E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide
CAS No.:78636-71-2
Molecular Formula:C₂₄H₂₁NO₂
Molecular Weight:355.436
Hs Code.:

Synonyms:(E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide

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Technology Process of (E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide

There total 1 articles about (E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 17812-07-6
Benzoylacrylic acid

: 103-49-1
dibenzylamine

: 78636-71-2
(E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide

Guidance literature:: Benzoylacrylic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -30 - 0 ℃; for 1h; Inert atmosphere; Schlenk technique;

dibenzylamine; In tetrahydrofuran; at -20 - 0 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201700541

Reference yield: 53.0%

: 78636-71-2
(E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide

: (-)-3-benzoyl-N,N-dibenzyloxirane-2-carboxamide

Guidance literature:: With C₃₄H₃₆F₆MnN₆O₆S₂; dihydrogen peroxide; acetic acid; In dichloromethane; acetonitrile; at -30 ℃; for 0.583333h; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201700541

Reference yield:

: 75-66-1
2-methylpropan-2-thiol

: 78636-71-2
(E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide

: C₂₈H₃₁NO₂S

: 1346164-42-8
C₂₈H₃₁NO₂S

Guidance literature:: (E)-N,N-dibenzyl-4-oxo-4-phenylbut-2-enamide; With C₂₈H₂₆F₆N₄S; In toluene; at 0 ℃; for 0.5h;

2-methylpropan-2-thiol; In toluene; at 0 ℃; for 96h; optical yield given as %ee;
DOI:10.1002/adsc.201100227