W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂

Base Information

Chemical Name:W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂
CAS No.:83634-33-7
Molecular Formula:C₁₇H₃₃Cl₂NP₂W
Molecular Weight:568.159
Hs Code.:

W(NC<sub>6</sub>H<sub>5</sub>)(CHC(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)2Cl<sub>2</sub>

Synonyms:W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂

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Chemical Property of W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂

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Technology Process of W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂

There total 2 articles about W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: tetra-t-butoxy(phenylimido)tungsten(VI)

: 70083-62-4
Ta(CHC(CH₃)3)(P(CH₃)3)2Cl₃

: 83634-33-7
W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂

: 2Ta⁽⁵⁺⁾*8(OC(CH₃)3)^(1-)*2Cl^(1-)=[Ta(OC(CH₃)3)4Cl]2

Guidance literature:: In diethyl ether; w and Ta complexes dissolved in Et2O under N2, reaction time 12 h; filtration, washing with pentane, drying in vac., recrystn. (toluene-pentane, -30°C), removal of solvent from filtrate, sublimation at 80°C, 0.001 mm Hg; elem. anal.;
DOI:10.1021/ja00390a016

Reference yield: 65.0%

: 83634-51-9
W(NC₆H₅)(CH₂C(CH₃)3)3Cl

: 10237-22-6
trimethyl phosphonium chloride

: 83634-33-7
W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂

Guidance literature:: With P(CH₃)3; In chloroform; P compds. added to soln. of W complex in CHCl3 under N2, mixture stirred and heated to 60°C for 24 h in glass bomb; filtration, evapn. in vac., recrystn. (toluene, -30°C); elem. anal.;
DOI:10.1021/ja00390a016

Reference yield: 95.0%

: 7446-70-0
aluminium trichloride

: 83634-33-7
W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl₂

: 83634-35-9
[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl]⁽¹⁺⁾*AlCl₄^(1-)=[W(NC₆H₅)(CHC(CH₃)3)(P(CH₃)3)2Cl]AlCl₄

Guidance literature:: In dichloromethane; W complex dissolved in CH2Cl2 under N2, AlCl3 added, mixture stirred for 0.5 h; filtration through Celite, concg. in vac., cooling to -30°C; elem. anal.;
DOI:10.1021/ja00390a016