3-<3-<(triphenylmethyl)amino>phenyl>-2-(2-hydroxybenzoyl)pentanoic acid tert-butyl ester

Base Information

Chemical Name:3-<3-<(triphenylmethyl)amino>phenyl>-2-(2-hydroxybenzoyl)pentanoic acid tert-butyl ester
CAS No.:166186-69-2
Molecular Formula:C₄₁H₄₁NO₄
Molecular Weight:611.781
Hs Code.:

Synonyms:3-<3-<(triphenylmethyl)amino>phenyl>-2-(2-hydroxybenzoyl)pentanoic acid tert-butyl ester

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Chemical Property of 3-<3-<(triphenylmethyl)amino>phenyl>-2-(2-hydroxybenzoyl)pentanoic acid tert-butyl ester

Chemical Property:

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Technology Process of 3-<3-<(triphenylmethyl)amino>phenyl>-2-(2-hydroxybenzoyl)pentanoic acid tert-butyl ester

There total 6 articles about 3-<3-<(triphenylmethyl)amino>phenyl>-2-(2-hydroxybenzoyl)pentanoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17408-16-1
3'-nitropropiophenone

: 166186-69-2
3-<3-<(triphenylmethyl)amino>phenyl>-2-(2-hydroxybenzoyl)pentanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) benzene, RT, 60 min, 2.) benzene, overnight

2: 4.15 g / H₂ / 5percent Pt/C / methanol / 2585.7 Torr

3: 8.75 g / diisopropylethylamine / CH₂Cl₂ / Ambient temperature

4: 1.) LDA / 1.) THF, hexane, -78 deg C, 50 min, 2.) THF, hexane, -78 deg C, 5 min

With hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; platinum on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jm00018a023

Reference yield:

: 62327-21-3
tert-butyl dimethylphosphonoacetate

: 166186-69-2
3-<3-<(triphenylmethyl)amino>phenyl>-2-(2-hydroxybenzoyl)pentanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) benzene, RT, 60 min, 2.) benzene, overnight

2: 4.15 g / H₂ / 5percent Pt/C / methanol / 2585.7 Torr

3: 8.75 g / diisopropylethylamine / CH₂Cl₂ / Ambient temperature

4: 1.) LDA / 1.) THF, hexane, -78 deg C, 50 min, 2.) THF, hexane, -78 deg C, 5 min

With hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; platinum on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jm00018a023

Reference yield:

: 3-(3-nitrophenyl)pent-2-enoic acid tert-butyl ester

: 166186-69-2
3-<3-<(triphenylmethyl)amino>phenyl>-2-(2-hydroxybenzoyl)pentanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 4.15 g / H₂ / 5percent Pt/C / methanol / 2585.7 Torr

2: 8.75 g / diisopropylethylamine / CH₂Cl₂ / Ambient temperature

3: 1.) LDA / 1.) THF, hexane, -78 deg C, 50 min, 2.) THF, hexane, -78 deg C, 5 min

With hydrogen; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; platinum on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jm00018a023