tert-butyl trans-[4-(4-trifluoromethanesulfonyloxyphenyl)cyclohexyloxy]acetate

Base Information

Chemical Name:tert-butyl trans-[4-(4-trifluoromethanesulfonyloxyphenyl)cyclohexyloxy]acetate
CAS No.:1239311-00-2
Molecular Formula:C₁₉H₂₅F₃O₆S
Molecular Weight:438.465
Hs Code.:

Synonyms:tert-butyl trans-[4-(4-trifluoromethanesulfonyloxyphenyl)cyclohexyloxy]acetate

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Chemical Property of tert-butyl trans-[4-(4-trifluoromethanesulfonyloxyphenyl)cyclohexyloxy]acetate

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Technology Process of tert-butyl trans-[4-(4-trifluoromethanesulfonyloxyphenyl)cyclohexyloxy]acetate

There total 4 articles about tert-butyl trans-[4-(4-trifluoromethanesulfonyloxyphenyl)cyclohexyloxy]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 1239310-99-6
tert-butyl trans-[4-(4-hydroxyphenyl)cyclohexyloxy]acetate

: 1239311-00-2
tert-butyl trans-[4-(4-trifluoromethanesulfonyloxyphenyl)cyclohexyloxy]acetate

Guidance literature:: With triethylamine; In dichloromethane; Cooling with ice;

Reference yield:

: 216880-00-1
trans-4-(4-allyloxyphenyl)cyclohexanol

: 1239311-00-2
tert-butyl trans-[4-(4-trifluoromethanesulfonyloxyphenyl)cyclohexyloxy]acetate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide; sodium hydroxide / water; toluene / 18 h

2: BARBITURIC ACID; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 3 h / Reflux

3: triethylamine / dichloromethane / Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; BARBITURIC ACID; tetrabutylammomium bromide; triethylamine; sodium hydroxide; In dichloromethane; water; toluene;

Reference yield:

: 65132-43-6
trans-4,4'-dihydroxy-cyclohexylbenzene

: 1239311-00-2
tert-butyl trans-[4-(4-trifluoromethanesulfonyloxyphenyl)cyclohexyloxy]acetate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide; acetone / 72 h

2: tetrabutylammomium bromide; sodium hydroxide / water; toluene / 18 h

3: BARBITURIC ACID; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 3 h / Reflux

4: triethylamine / dichloromethane / Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; BARBITURIC ACID; tetrabutylammomium bromide; potassium carbonate; triethylamine; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;